Аннотации:
Методом рентгеноструктурного анализа (РСА) определено строение восьми органических
и элементоорганических соединений. РСА соединений проводили на автоматическом
четырехкружном дифрактометре D8 Quest Bruker (МоКа-излучение, X = 0,71073 А, графитовый монохроматор) при 293 К. Соединение [Ph3PMe] [RuCl4(DMSO)2] (1) P-1, a = 8,4181(3), b = 8,9389(3), c = 11,1396(4) А, a = 69,754(1), P = 81,913(2), у = 64,491(1) град., V = 709,75(4) А3, Z = 1. [Ph3PC6H4CH2CN] Cl • CHCl3 (2), P 21/n, a = 9,846(6) А, b = 15,782(14) А, c = 15,111(10) А, a = 90, P = 91,027(18), у = 90 град., V = 2348(3) А3, Z = 4. Ph4SbOC6H4(NO2-4) (3), P-1, a = 11,101(6), b = 12,684(6), c = 19,359(9) А, a = 80,973(17), в = 80,17(2), у = 72,31(3) град., V = 2543(2) А3, Z = 4. (4-BrC6H4)3Sb (4), P-1, a = 6,273(12), b = 12,83(2), c = 13,26(3) А, a = 78,67(8), P = 84,33(9), у = 80,81(7) град., V = 1031(3) А3, Z = 2. Ph4PBrH2O (5), P-1, a = 10,025(10), b = 10,676(10), c = 10,706(13) А, a = 77,56(4), P = 71,80(4), у = 83,26(3) град., V = 1061(2) А3, Z = 2. [4-MeOC6H4]3Sb (6), P-3, a = 13,27(3), b = 13,27(3), c = 19,24(7) А, a = 77,56(4), P = 90, у = 120 град., V = 2935(20) А3, Z = 6. [Ph3PCH2C6H4CN-4]Cl, P 21/n, a = 9,456(6), b = 14,733(9), c = 16,271(9) А, a = 90, P = 104,83(2), у = 90 град., V = 2191(2) А3, Z = 4. [Ph3PCH2OH]Cl, P 21/c, a = 8,888(9), b = 17,795(19), c = 11,278(12) А, a = 90, P = 99,52(4), у = 90 град., V = 1759(3) А3, Z = 4. The structure of eight organic and organoelemental compounds was determined by X-ray structural analysis (XRD). XRD analysis of compounds was performed on an automatic four- circle diffractometer D8 Quest Bruker (МоАа, 1 = 0,71073 A, 293 К. 1 (C23H30Cl4O2PRuS2, P-1, a = 8.4181(3), b = 8.9389(3), c = 11.1396(4) A, а = 69.754(1), в = 81.913(2), у = 64.491(1) deg., V = 709.75(4) A3, Z =1. 2 (C21H18Cl4NP, P 21/n, a = 9.846(6) A, b = 15.782(14) A, c = 15.111(10) A, а = 90, в = 91.027(18), у = 90 deg., V = 2348(3) A3, Z = 4. 3 (C30H24NO3Sb, P-1, a = 11.101(6), b = 12.684(6), c = 19.359(9) A, а = 80.973(17), в = 80.17(2), у = 72.31(3) deg., V = 2543(2) A3, Z = 4. 4 (C21H15Br3Sb, P-1, a = 6.273(12), b = 12.83(2), c = 13.26(3) A, а = 78.67(8), в = 84.33(9), у= 80.81(7) deg., V = 1031(3) A3, Z = 2. 5 (C24H22BrOP, P-1, a = 10.025(10), b = 10.676(10), c = 10.706(13) A, а = 77.56(4), в = 71.80(4), у = 83.26(3) deg., V= 1061(2) A3, Z = 2. 6 (C21H21O3Sb, R-3, a = 13.27(3), b = 13.27(3), c = 19.24(7) A, а = 77.56(4), в = 90, у = 120 deg., V= 2935(20) A3, Z = 6. 7 (C26H21ClNP, P 21/n, a = 9.456(6), b = 14.733(9), c = 16.271(9) A, а = 90, в = 104.83(2), у = 90 deg., V = 2191(2) A3, Z = 4. 8 (C19H18ClOP, P 21/c, a = 8.888(9), b = 17.795(19), c = 11.278(12) A, а = 90, в = 99.52(4), у = 90 deg., V = 1759(3) A3, Z = 4.